International
Tables for
Crystallography
Volume C
Mathematical, physical and chemical tables
Edited by E. Prince

International Tables for Crystallography (2006). Vol. C. ch. 4.4, pp. 437-438

Section 4.4.2.4.4. Capillary optics

I. S. Andersona and O. Schärpff

4.4.2.4.4. Capillary optics

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Capillary neutron optics, in which hollow glass capillaries act as waveguides, are also based on the concept of total external reflection of neutrons from a smooth surface. The advantage of capillaries, compared with neutron guides, is that the channel sizes are of the order of a few tens of micrometres, so that the radius of curvature can be significantly decreased for a given characteristic wavelength [see equation (4.4.2.6)[link]]. Thus, neutrons can be efficiently deflected through large angles, and the device can be more compact.

Two basic types of capillary optics exist, and the choice depends on the beam characteristics required. Polycapillary fibres are manufactured from hollow glass tubes several centimetres in diameter, which are heated, fused and drawn multiple times until bundles of thousands of micrometre-sized channels are formed having an open area of up to 70% of the cross section. Fibre outer diameters range from 300 to 600 µm and contain hundreds or thousands of individual channels with inner diameters between 3 and 50 µm. The channel cross section is usually hexagonal, though square channels have been produced, and the inner channel wall surface roughness is typically less than 10 Å r.m.s., giving rise to very high reflectivities. The principal limitations on transmission efficiency are the open area, the acceptable divergence (note that the critical angle for glass is 1 mrad Å−1) and reflection losses due to absorption and scattering. A typical optical device will comprise hundreds or thousands of fibres threaded through thin screens to produce the required shape.

Fig. 4.4.2.6[link] shows typical applications of polycapillary devices. In Fig. 4.4.2.6[link](a), a polycapillary lens is used to refocus neutrons collected from a divergent source. The half lens depicted in Fig. 4.4.2.6[link](b) can be used either to produce a nearly parallel (divergence = [2\gamma _{c}]) beam from a divergent source or (in the reverse sense) to focus a nearly parallel beam, e.g. from a neutron guide. The size of the focal point depends on the channel size, the beam divergence, and the focal length of the lens. For example, a polycapillary lens used in a prompt γ-activation analysis instrument at the National Institute of Standards and Technology to focus a cold neutron beam from a neutron guide results in a current density gain of 80 averaged over the focused beam size of 0.53 mm (Chen et al., 1995[link]).

[Figure 4.4.2.6]

Figure 4.4.2.6| top | pdf |

Typical applications of polycapillary devices: (a) lens used to refocus a divergent beam; (b) half-lens to produce a nearly parallel beam or to focus a nearly parallel beam; (c) a compact bender.

Fig. 4.4.2.6(c)[link] shows another simple application of polycapillaries as a compact beam bender. In this case, such a bender may be more compact than an equivalent multichannel guide bender, although the accepted divergence will be less. Furthermore, as with curved neutron guides, owing to the wavelength dependence of the critical angle the capillary curvature can be used to filter out thermal or high-energy neutrons.

It should be emphasized that the applications depicted in Fig. 4.4.2.6[link] obey Liouville's theorem, in that the density of neutrons in phase space is not changed, but the shape of the phase-space volume is altered to meet the requirements of the experiment, i.e. there is a simple trade off between beam dimension and divergence.

The second type of capillary optic is a monolithic configuration. The individual capillaries in monolithic optics are tapered and fused together, so that no external frame assembly is necessary (Chen-Mayer et al., 1996[link]). Unlike the multifibre devices, the inner diameters of the channels that make up the monolithic optics vary along the length of the component, resulting in a smaller more compact design.

Further applications of capillary optics include small-angle scattering (Mildner, 1994[link]) and lenses for high-spatial-resolution area detection.

References

First citation Chen, H., Sharov, V. A., Mildner, D. F. R., Downing, R. G., Paul, R. L., Lindstrom, R. M., Zeissler, C. J. & Xiao, Q. F. (1995). Prompt gamma activation analysis enhanced by a neutron focusing capillary lens. Nucl. Instrum. Methods, B95, 107–114.Google Scholar
First citation Chen-Mayer, H. H., Mildner, D. F. R., Sharov, V. A., Ullrich, J. B., Ponomarev, I. Yu. & Downing, R. G. (1996). Monolithic polycapillary neutron focusing lenses: experimental characterizations. J. Phys. Soc. Jpn, 65, Suppl. A, 319–321.Google Scholar
First citation Mildner, D. F. R. (1994). Neutron focusing optics for low-resolution small-angle scattering. J. Appl. Cryst. 27, 521–526.Google Scholar








































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