International
Tables for
Crystallography
Volume C
Mathematical, physical and chemical tables
Edited by E. Prince

International Tables for Crystallography (2006). Vol. C. ch. 7.1, p. 618

Section 7.1.1.2. Densitometry

P. M. de Wolfff

7.1.1.2. Densitometry

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If the blackening is measured with a microdensitometer, an accuracy of 0.002 density units up to densities of at least 2 is easily attained. Higher precision is rarely required, as the limiting factors are graininess of the film and irregularities in the emulsion and processing. The grains in processed X-ray film are larger than those produced by visible light, and occur in clusters around each absorbed quantum. The resulting statistical fluctuations may be minimized by appropriate choice of densitometer slit dimensions and scanning speed. If the X-rays are not incident normally on double-coated film, it may be necessary to make corrections for obliquity (Whittaker, 1953[link]; Hellner, 1954[link]).

References

First citation Hellner, E. (1954). Intensitätsmessungen aus Aufnahmen in der Guinier-Kamera. Z. Kristallogr. 106, 122–145.Google Scholar
First citation Whittaker, E. J. W. (1953). The Cox & Shaw factor. Acta Cryst. 6, 218.Google Scholar








































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