International
Tables for Crystallography Volume C Mathematical, physical and chemical tables Edited by E. Prince © International Union of Crystallography 2006 |
International Tables for Crystallography (2006). Vol. C. ch. 7.1, p. 618
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If the blackening is measured with a microdensitometer, an accuracy of 0.002 density units up to densities of at least 2 is easily attained. Higher precision is rarely required, as the limiting factors are graininess of the film and irregularities in the emulsion and processing. The grains in processed X-ray film are larger than those produced by visible light, and occur in clusters around each absorbed quantum. The resulting statistical fluctuations may be minimized by appropriate choice of densitometer slit dimensions and scanning speed. If the X-rays are not incident normally on double-coated film, it may be necessary to make corrections for obliquity (Whittaker, 1953; Hellner, 1954).
References
Hellner, E. (1954). Intensitätsmessungen aus Aufnahmen in der Guinier-Kamera. Z. Kristallogr. 106, 122–145.Google ScholarWhittaker, E. J. W. (1953). The Cox & Shaw factor. Acta Cryst. 6, 218.Google Scholar