International Tables for Crystallography (2006). Vol. F, ch. 10.1, pp. 197-201   | 1 | 2 |
doi: 10.1107/97809553602060000672

Chapter 10.1. Introduction to cryocrystallography

Contents

  • 10.1. Introduction to cryocrystallography  (pp. 197-201) | html | pdf | chapter contents |
    • 10.1.1. Utility of low-temperature data collection  (p. 197) | html | pdf |
      • 10.1.1.1. Prevention of radiation damage  (p. 197) | html | pdf |
      • 10.1.1.2. Mechanical stability of the crystal mount  (p. 197) | html | pdf |
      • 10.1.1.3. Effect on resolution  (p. 197) | html | pdf |
    • 10.1.2. Cooling of biocrystals  (pp. 197-199) | html | pdf |
      • 10.1.2.1. Physical chemistry of biocrystals  (pp. 197-198) | html | pdf |
      • 10.1.2.2. Internal ice or phase transition  (p. 198) | html | pdf |
      • 10.1.2.3. Removal of the solvent layer  (p. 198) | html | pdf |
      • 10.1.2.4. Cooling rates  (pp. 198-199) | html | pdf |
    • 10.1.3. Principles of cooling equipment  (p. 199) | html | pdf |
      • 10.1.3.1. Cold gas supply  (p. 199) | html | pdf |
      • 10.1.3.2. Frost prevention  (p. 199) | html | pdf |
    • 10.1.4. Operational considerations  (pp. 199-201) | html | pdf |
      • 10.1.4.1. Dual-stream instruments  (pp. 199-200) | html | pdf |
      • 10.1.4.2. Electrically heated nozzle  (pp. 200-201) | html | pdf |
      • 10.1.4.3. Temperature calibration  (p. 201) | html | pdf |
      • 10.1.4.4. Transfer of the crystal to the diffractometer  (p. 201) | html | pdf |
    • 10.1.5. Concluding note  (p. 201) | html | pdf |
    • References | html | pdf |
    • Figures
      • Fig. 10.1.4.1. Schematic drawing of a dual-stream setup with the streams parallel to the diffractometer ϕ axis  (p. 199) | html | pdf |
      • Fig. 10.1.4.2. Schematic drawing of a dual-stream setup with the streams angled relative to the diffractometer ϕ axis  (p. 200) | html | pdf |
      • Fig. 10.1.4.3. Schematic drawing of a single-stream setup with the stream parallel to the diffractometer ϕ axis  (p. 200) | html | pdf |
      • Fig. 10.1.4.4. Schematic drawing of a single-stream setup with the stream angled relative to the diffractometer ϕ axis  (p. 200) | html | pdf |