International
Tables for Crystallography Volume C Mathematical, physical and chemical tables Edited by E. Prince © International Union of Crystallography 2006 |
International Tables for Crystallography (2006). Vol. C. ch. 4.2, pp. 236-237
Section 4.2.5.2.1. Mirrors
D. C. Creaghb
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In the laboratory, mirrors are used in conjunction with conventional sealed tubes and rotating-anode sources, the emission from which consists of Bremsstrahlung upon which is superimposed the characteristic spectrum of the anode material (Subsection 2.3.5.2 ). The shape of the Bremsstrahlung spectrum can be significantly modified by mirrors, and the intensity emitted at harmonics of the characteristic wavelength can be significantly reduced. More importantly, the mirrors can be fashioned into shapes that enable the emitted radiation to be brought to a focus. Ellipsoidal, logarithmic spiral, and toroidal mirrors have been manufactured commercially for use with laboratory X-ray sources. Since the X-rays are emitted isotropically from the anode surface, it is important to devise a mirror system that has a maximum angle of acceptance and a relatively long focal length.
At synchrotron-radiation sources, the high intensities that are generated over a very broad spectral range give rise to significant heat loading of subsequent monochromators and therefore degrade the performance of these elements. In many systems, mirrors are used as the first optical element in the monochromator, to reduce the heat load on the primary monochromator and to make it easier for the subsequent monochromators to reject harmonics of the chosen radiation. Shaped mirror geometries are often used to focus the beam in the horizontal plane (Subsection 2.2.7.3 ). A schematic diagram of the optical elements of a typical synchrotron-radiation beamline is shown in Fig. 4.2.5.2 . In this, the primary mirror acts as a thermal shunt for the subsequent monochromator, minimizes the high-energy component that may give rise to possible harmonic content in the final beam, and acts as a vertical collimator. The radii of curvature of mirrors can be changed using a mechanical four-point bending system (Oshima, Harada & Sakabe, 1986). More recent advances in mirror technology enable the shape of the mirror to be changed through use of the piezoelectric effect (Sussini & Labergerie, 1995).
References
Oshima, K., Harada, J. & Sakabe, N. (1986). Curved crystal monochromator. X-ray instrumentation for the Photon Factory: dynamic analyses of micro-structures in matter, edited by S. Hosoya, Y. Iitaka & H. Hashizume, pp. 35–41. Japan: Photon Factory.Google ScholarSussini, J. & Labergerie, D. (1995). Bi-morph piezo-electric mirror: a novel active mirror. Synchrotron Rad. News, 8, 21–26.Google Scholar