International
Tables for Crystallography Volume C Mathematical, physical and chemical tables Edited by E. Prince © International Union of Crystallography 2006 |
International Tables for Crystallography (2006). Vol. C. ch. 4.4, p. 431
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Figure 4.4.1.2
Schematic diagram for performing diffraction experiments at steady-state and pulsed neutron sources. On the left we see the familiar monochromator crystal allowing a constant (in time) beam to fall on the sample (centre left), which then diffracts the beam through an angle 2θs into the detector. The signal in the latter is also constant in time (lower left). On the right, the pulsed source allows a wide spectrum of neutrons to fall on the sample in sharp pulses separated by Δt (centre right). The neutrons are then diffracted by the sample through 2θs and their time of arrival in the detector is analysed (lower right). The centre figure shows the time-averaged flux at the source. At a reactor, we make use of a narrow band of neutrons (heavy shading), here chosen with λ = 1.5 Å. At a pulsed source, we use a wide spectral band, here chosen from 0.4 to 3 Å and each one is identified by its time-of-flight. For the experimentalist, an important parameter is the integrated area of the two-shaded areas. Here they have been made identical. |