Accuracy in Rietveld quantitative phase analysis with strictly monochromatic Mo and Cu radiations
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
ch. 3.10,
pp. 374-384
[ doi:10.1107/97809553602060000955 ]
mode (
Cuesta et al., 2015). Mo radiation combined with a flat sample in transmission geometry allows an irradiated volume of close to 100 mm 3 ; meanwhile, for Cu radiation (flat samples in reflection and transmission geometries ...
Conclusions
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.10,
pp. 383-384
[ doi:10.1107/97809553602060000955 ]
methods. J. Solid State Chem. 117, 165–176. Google Scholar
Brown, G. M. & Levy, H. A. (1979). α- D -Glucose: further refinement based on neutron-diffraction data. Acta Cryst. B 35, 656–659. Google Scholar
Cuesta ...
Variable amorphous content series
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.2.4,
pp. 375-376
[ doi:10.1107/97809553602060000955 ]
by adding ∼20 wt% quartz (Q) as an internal standard.
References
García-Maté, M., Santacruz, I.,
Cuesta, A., León-Reina, L., Aranda, M. A. G., Baco, I., Morin, V., Walenta, G., Gartner, E. & De la Torre, A. G. (2014). Amorphous ...
[
more
results from section 3.10.2 in volume H]
Transmission synchrotron X-ray powder diffraction (SXRPD)
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.3.3,
pp. 376-377
[ doi:10.1107/97809553602060000955 ]
[
more
results from section 3.10.3 in volume H]
Increasing crystalline organic phase content series
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.8,
pp. 381-382
[ doi:10.1107/97809553602060000955 ]
Increasing inorganic crystalline phase content series
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.7,
pp. 381-381
[ doi:10.1107/97809553602060000955 ]
3.10.6). As a consequence, the refined values for flat samples in reflection and transmission geometries were smaller and larger than 1.0, respectively (
Cuesta et al., 2015). Although preferred orientation is present in all patterns, the Cu ...
Introduction
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.1,
pp. 374-375
[ doi:10.1107/97809553602060000955 ]
3.10.1 (a) and 3.10.1 (b) show the irradiated volumes bathed by X-rays when using flat samples for Mo and Cu radiations in transmission geometry, and Fig. 3.10.1 (c) shows the irradiated volume for Cu in reflection mode (
Cuesta et ...
Increasing amorphous content series within an inorganic crystalline phase matrix
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.9,
pp. 382-383
[ doi:10.1107/97809553602060000955 ]
Powder-diffraction data analysis
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.4,
pp. 377-377
[ doi:10.1107/97809553602060000955 ]
Crystalline single phases
León-Reina, L.,
Cuesta, A.,
García-Maté, M.,
Álvarez-Pinazo, G.,
Santacruz, I.,
Vallcorba, O.,
De la Torre, A.G. and
Aranda, M.A.G.,
International Tables for Crystallography
(2019).
Vol. H,
Section 3.10.5,
pp. 377-379
[ doi:10.1107/97809553602060000955 ]
