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Accuracy in Rietveld quantitative phase analysis with strictly monochromatic Mo and Cu radiations
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, ch. 3.10, pp. 374-384 [ doi:10.1107/97809553602060000955 ]
... analysis (RQPA) results can be gathered into three main groups: (i) instrument related, (ii) sample-preparation related and (iii) data-analysis ... of microabsorption effects. High-energy (short-wavelength) X-rays contribute (i) to minimize absorption and microabsorption effects, (ii) to the measurement ... Leibler distance (KLD; Kullback, 1968 ). The three series were (i) crystalline inorganic phase mixtures with increasing amounts of an ...

Increasing amorphous content series within an inorganic crystalline phase matrix
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.9, pp. 382-383 [ doi:10.1107/97809553602060000955 ]
... n-Reina, L., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A. G. & Aranda, M. A. ...

Increasing crystalline organic phase content series
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.8, pp. 381-382 [ doi:10.1107/97809553602060000955 ]
... n-Reina, L., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A. G. & Aranda, M. A. ...

Increasing inorganic crystalline phase content series
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.7, p. 381 [ doi:10.1107/97809553602060000955 ]
... RQPA results for six inorganic mixtures with increasing amounts of i-A measured with MoK[alpha]1 (transmission) and CuK[alpha ... reflection). The Rietveld plots of the mixture with 4wt% i-A are shown in Fig. 3.10.6 . For most of ... distance (AKLD) for each mixture and the KLD value for i-anhydrite are also included. Trm, transmission; rfl, reflection. CGpQ_ ...

Limits of detection and quantification
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.6, pp. 379-381 [ doi:10.1107/97809553602060000955 ]
... squares) and Fig. 3.10.4 shows the strongest diffraction peak for i-A in the mixtures containing 0.123wt% anhydrite (CGpQ_0.12A) and ... respectively. Hence, it can be concluded that the LoD for i-A with this radiation in this mixture is quite close ... pattern, arises from SrSO4 (0.39wt%) from gypsum. The LoQ for i-A in this matrix was also studied. Three MoK[ ...

Crystalline single phases
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.5, pp. 377-379 [ doi:10.1107/97809553602060000955 ]
... n-Reina, L., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A. G. & Aranda, M. A. ...

Powder-diffraction data analysis
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.4, p. 377 [ doi:10.1107/97809553602060000955 ]
... of Portland cements. J. Appl. Cryst. 42, 906-916.GoogleScholar Madsen, I. C., Scarlett, N. V. Y., Cranswick, L. M. D. & Lwin ... 1a to 1h. J. Appl. Cryst. 34, 409-426.GoogleScholar Madsen, I. C., Scarlett, N. V. Y. & Kern, A. (2011). Description ... Z. Kristallogr. 226, 944-955.GoogleScholar Scarlett, N. V. Y., Madsen, I. C., Cranswick, L. M. D., Lwin, T., Groleau, E., ...

Transmission synchrotron X-ray powder diffraction (SXRPD)
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.3.3, pp. 376-377 [ doi:10.1107/97809553602060000955 ]
... wavelength was [lambda] = 0.49591(2)Å. References Fauth, F., Peral, I., Popescu, C. & Knapp, M. (2013). The new material science ...
     [more results from section 3.10.3 in volume H]

Variable amorphous content series
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.2.4, pp. 375-376 [ doi:10.1107/97809553602060000955 ]
... Q) as an internal standard. References García-Maté, M., Santacruz, I., Cuesta, A., León-Reina, L., Aranda, M. A. G., Baco, I., Morin, V., Walenta, G., Gartner, E. & De la Torre, ...
     [more results from section 3.10.2 in volume H]

Introduction
León-Reina, L., Cuesta, A., García-Maté, M., Álvarez-Pinazo, G., Santacruz, I., Vallcorba, O., De la Torre, A.G. and Aranda, M.A.G.  International Tables for Crystallography (2019). Vol. H, Section 3.10.1, pp. 374-375 [ doi:10.1107/97809553602060000955 ]
... analysis (RQPA) results can be gathered into three main groups: (i) instrument related, (ii) sample-preparation related and (iii) data-analysis ... of microabsorption effects. High-energy (short-wavelength) X-rays contribute (i) to minimize absorption and microabsorption effects, (ii) to the measurement ... Leibler distance (KLD; Kullback, 1968 ). The three series were (i) crystalline inorganic phase mixtures with increasing amounts of an ...

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