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Quantitative texture analysis and combined analysis
International Tables for Crystallography (2019). Vol. H, ch. 5.3, pp. 555-580 [ doi:10.1107/97809553602060000968 ]
... to the mollusc shell growth, margin and normal directions (G, M and N, respectively). In thin-film analyses (Chateigner & Erler ... the case of unidirectional experimental environments such as magnetic fields (Morales et al., 2003 ), fibre spinning, axial pressure (Wenk et al. ... an extension of the WIMV method (Lutterotti et al., 2004 ; Morales et al., 2002 ). In this latter the OD ...
Examination of a solution
International Tables for Crystallography (2019). Vol. H, Section 5.3.5.6, pp. 577-578 [ doi:10.1107/97809553602060000968 ]
Examination of a solution 5.3.5.6. Examination of a solution Using single-pattern refinement, a simple examination of the modelled and measured diagrams can suffice to detect refinement problems or refinement quality. When several hundreds of patterns are refined, such a comparison is cumbersome or simply impossible. One possibility to rapidly check ...
[more results from section 5.3.5 in volume H]
Remarks
International Tables for Crystallography (2019). Vol. H, Section 5.3.4.7, pp. 570-571 [ doi:10.1107/97809553602060000968 ]
... Cryst. 26, 449-452.GoogleScholar Cerný, R., Valvoda, V. & Chládek, M. (1995). Empirical texture corrections for asymmetric diffraction and inclined ...
[more results from section 5.3.4 in volume H]
An example
International Tables for Crystallography (2019). Vol. H, Section 5.3.3.3, pp. 568-569 [ doi:10.1107/97809553602060000968 ]
An example 5.3.3.3. An example Here, we illustrate magnetic quantitative texture analysis on an iron sample exhibiting magnetic saturation around 0.5T (Chateigner et al., 2010 ) that was initially not magnetized. Measurements were carried out on the D19 beamline at ILL first without and then with an applied magnetic field of 0.3T ...
[more results from section 5.3.3 in volume H]
Reciprocal-space mapping
International Tables for Crystallography (2019). Vol. H, Section 5.3.2.8, pp. 566-567 [ doi:10.1107/97809553602060000968 ]
Reciprocal-space mapping 5.3.2.8. Reciprocal-space mapping Reciprocal-space mapping (RSM) represents the localization of the momentum transfer in the sample reference frame (KA). The momentum-transfer vector q is defined by in which ki and ko are the incident and outgoing wavevectors, respectively. The goal of RSM is then ...
[more results from section 5.3.2 in volume H]
Introduction
International Tables for Crystallography (2019). Vol. H, Section 5.3.1, p. 555 [ doi:10.1107/97809553602060000968 ]
... often determines the characteristics of the sample. References Rietveld, H. M. (1969). A profile refinement method for nuclear and magnetic ...
Conclusions
International Tables for Crystallography (2019). Vol. H, Section 5.3.6, p. 578 [ doi:10.1107/97809553602060000968 ]
Conclusions 5.3.6. Conclusions Classical quantitative texture analysis (and also residual stress, line broadening, phase composition etc.) becomes of questionable value for real samples that exhibit complex architectures with several phases and strong intra- and inter-phase peak overlapping. This is particularly true for poorly crystallized or nanocrystallized samples, for which line ...
International Tables for Crystallography (2019). Vol. H, ch. 5.3, pp. 555-580 [ doi:10.1107/97809553602060000968 ]
... to the mollusc shell growth, margin and normal directions (G, M and N, respectively). In thin-film analyses (Chateigner & Erler ... the case of unidirectional experimental environments such as magnetic fields (Morales et al., 2003 ), fibre spinning, axial pressure (Wenk et al. ... an extension of the WIMV method (Lutterotti et al., 2004 ; Morales et al., 2002 ). In this latter the OD ...
Examination of a solution
International Tables for Crystallography (2019). Vol. H, Section 5.3.5.6, pp. 577-578 [ doi:10.1107/97809553602060000968 ]
Examination of a solution 5.3.5.6. Examination of a solution Using single-pattern refinement, a simple examination of the modelled and measured diagrams can suffice to detect refinement problems or refinement quality. When several hundreds of patterns are refined, such a comparison is cumbersome or simply impossible. One possibility to rapidly check ...
[more results from section 5.3.5 in volume H]
Remarks
International Tables for Crystallography (2019). Vol. H, Section 5.3.4.7, pp. 570-571 [ doi:10.1107/97809553602060000968 ]
... Cryst. 26, 449-452.GoogleScholar Cerný, R., Valvoda, V. & Chládek, M. (1995). Empirical texture corrections for asymmetric diffraction and inclined ...
[more results from section 5.3.4 in volume H]
An example
International Tables for Crystallography (2019). Vol. H, Section 5.3.3.3, pp. 568-569 [ doi:10.1107/97809553602060000968 ]
An example 5.3.3.3. An example Here, we illustrate magnetic quantitative texture analysis on an iron sample exhibiting magnetic saturation around 0.5T (Chateigner et al., 2010 ) that was initially not magnetized. Measurements were carried out on the D19 beamline at ILL first without and then with an applied magnetic field of 0.3T ...
[more results from section 5.3.3 in volume H]
Reciprocal-space mapping
International Tables for Crystallography (2019). Vol. H, Section 5.3.2.8, pp. 566-567 [ doi:10.1107/97809553602060000968 ]
Reciprocal-space mapping 5.3.2.8. Reciprocal-space mapping Reciprocal-space mapping (RSM) represents the localization of the momentum transfer in the sample reference frame (KA). The momentum-transfer vector q is defined by in which ki and ko are the incident and outgoing wavevectors, respectively. The goal of RSM is then ...
[more results from section 5.3.2 in volume H]
Introduction
International Tables for Crystallography (2019). Vol. H, Section 5.3.1, p. 555 [ doi:10.1107/97809553602060000968 ]
... often determines the characteristics of the sample. References Rietveld, H. M. (1969). A profile refinement method for nuclear and magnetic ...
Conclusions
International Tables for Crystallography (2019). Vol. H, Section 5.3.6, p. 578 [ doi:10.1107/97809553602060000968 ]
Conclusions 5.3.6. Conclusions Classical quantitative texture analysis (and also residual stress, line broadening, phase composition etc.) becomes of questionable value for real samples that exhibit complex architectures with several phases and strong intra- and inter-phase peak overlapping. This is particularly true for poorly crystallized or nanocrystallized samples, for which line ...
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