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Results for DC.creator="D." AND DC.creator="C." AND DC.creator="Phillips" in section 25.1.2 of volume F page 1 of 2 pages. |
Structure analysis at 6Å resolution
International Tables for Crystallography (2012). Vol. F, Section 25.1.2, pp. 845-854 [ doi:10.1107/97809553602060000899 ]
... had been built in the laboratory to the design of D. A. G. Broad (patent 1956) under the direction of U. ... In addition, we had a laboratory prototype linear diffractometer (Arndt & Phillips, 1961), which had been made in the laboratory workshop by ... that the unit-cell dimensions were a = b = 79.1Å and c = 37.9Å, and that the space group was or (Corey ...
Phase determination at 6Å resolution
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.7, p. 852 [ doi:10.1107/97809553602060000899 ]
... these minor sites were not taken into account. References Blow, D. M. & Crick, F. H. C. (1959). The treatment of errors in the isomorphous replacement method. Acta Cryst. 12, 794-802. Blow, D. M. & Rossmann, M. G. (1961). The single isomorphous ...
Re-assessment of heavy-atom derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.4, pp. 851-852 [ doi:10.1107/97809553602060000899 ]
... appear at reduced weight in a complex background (Blow, 1958; Phillips, 1966). Nevertheless, the maps for PdCl4 and MHTS were ... 0, 1, 2kl reflections only. ++hk0 reflections only. References Blow, D. M. (1958). The structure of haemoblobin. VII. Determination of ... other than relative y's. Acta Cryst. 14, 1194-1195. Phillips, D. C. (1966). The three-dimensional structure of ...
The absolute scale of the intensities
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.3, p. 851 [ doi:10.1107/97809553602060000899 ]
... R. Soc. London Ser. A, 258, 181. Wilson, A. J. C. (1942). Determination of absolute from relative X-ray intensity ...
Data processing
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.2, pp. 850-851 [ doi:10.1107/97809553602060000899 ]
... when more than one estimation was available. References Hamilton, W. C. (1955). On the treatment of unobserved reflexions in the ... of crystal structures. Acta Cryst. 8, 185-186. North, A. C. T. (1964). Computer processing of automatic diffractometer data. J. ...
X-ray intensity measurements
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.1, pp. 848-850 [ doi:10.1107/97809553602060000899 ]
... available and, third, there was the prototype linear diffractometer (Arndt & Phillips, 1961). We chose the last option, since CCFB, RHF ... origin of the reciprocal lattice. A'OA, B'OB and C'OC are the principal axes of the reciprocal lattice, here ... reflection. The reciprocal lattice can be rotated about the axis C'OC, and this axis can be inclined to the ...
Analysis in three dimensions
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6, pp. 848-852 [ doi:10.1107/97809553602060000899 ]
... available and, third, there was the prototype linear diffractometer (Arndt & Phillips, 1961). We chose the last option, since CCFB, RHF ... origin of the reciprocal lattice. A'OA, B'OB and C'OC are the principal axes of the reciprocal lattice, here ... reflection. The reciprocal lattice can be rotated about the axis C'OC, and this axis can be inclined to the ...
Refinement of heavy-atom parameters
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.5, p. 848 [ doi:10.1107/97809553602060000899 ]
Refinement of heavy-atom parameters 25.1.2.5. Refinement of heavy-atom parameters Refinement of the heavy-atom parameters was first performed by the use of Rollett's (1961) least-squares program on the MERCURY computer, using the values as structure amplitudes. This procedure gave satisfactory results for the K2HgI4, K2PdCl4 and MHTS ...
Other potential derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.4, pp. 847-848 [ doi:10.1107/97809553602060000899 ]
Other potential derivatives 25.1.2.4.4. Other potential derivatives As is usual in protein work, RJP tried many other heavy-atom compounds (Poljak, 1963), but none gave useful results. In particular, a uranyl derivative, obtained by the use of UO2NO3, gave difference-Patterson maps that were difficult to interpret, and it was not ...
The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.3, p. 847 [ doi:10.1107/97809553602060000899 ]
The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative 25.1.2.4.3. The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative The hk0 difference-Patterson map of the p-mercuribenzene sulfonate (PCMBS) derivative was interpretable in terms of a single site of substitution at 8Å resolution, but it was not useful beyond about 8 Å because of lack ...
International Tables for Crystallography (2012). Vol. F, Section 25.1.2, pp. 845-854 [ doi:10.1107/97809553602060000899 ]
... had been built in the laboratory to the design of D. A. G. Broad (patent 1956) under the direction of U. ... In addition, we had a laboratory prototype linear diffractometer (Arndt & Phillips, 1961), which had been made in the laboratory workshop by ... that the unit-cell dimensions were a = b = 79.1Å and c = 37.9Å, and that the space group was or (Corey ...
Phase determination at 6Å resolution
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.7, p. 852 [ doi:10.1107/97809553602060000899 ]
... these minor sites were not taken into account. References Blow, D. M. & Crick, F. H. C. (1959). The treatment of errors in the isomorphous replacement method. Acta Cryst. 12, 794-802. Blow, D. M. & Rossmann, M. G. (1961). The single isomorphous ...
Re-assessment of heavy-atom derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.4, pp. 851-852 [ doi:10.1107/97809553602060000899 ]
... appear at reduced weight in a complex background (Blow, 1958; Phillips, 1966). Nevertheless, the maps for PdCl4 and MHTS were ... 0, 1, 2kl reflections only. ++hk0 reflections only. References Blow, D. M. (1958). The structure of haemoblobin. VII. Determination of ... other than relative y's. Acta Cryst. 14, 1194-1195. Phillips, D. C. (1966). The three-dimensional structure of ...
The absolute scale of the intensities
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.3, p. 851 [ doi:10.1107/97809553602060000899 ]
... R. Soc. London Ser. A, 258, 181. Wilson, A. J. C. (1942). Determination of absolute from relative X-ray intensity ...
Data processing
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.2, pp. 850-851 [ doi:10.1107/97809553602060000899 ]
... when more than one estimation was available. References Hamilton, W. C. (1955). On the treatment of unobserved reflexions in the ... of crystal structures. Acta Cryst. 8, 185-186. North, A. C. T. (1964). Computer processing of automatic diffractometer data. J. ...
X-ray intensity measurements
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6.1, pp. 848-850 [ doi:10.1107/97809553602060000899 ]
... available and, third, there was the prototype linear diffractometer (Arndt & Phillips, 1961). We chose the last option, since CCFB, RHF ... origin of the reciprocal lattice. A'OA, B'OB and C'OC are the principal axes of the reciprocal lattice, here ... reflection. The reciprocal lattice can be rotated about the axis C'OC, and this axis can be inclined to the ...
Analysis in three dimensions
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.6, pp. 848-852 [ doi:10.1107/97809553602060000899 ]
... available and, third, there was the prototype linear diffractometer (Arndt & Phillips, 1961). We chose the last option, since CCFB, RHF ... origin of the reciprocal lattice. A'OA, B'OB and C'OC are the principal axes of the reciprocal lattice, here ... reflection. The reciprocal lattice can be rotated about the axis C'OC, and this axis can be inclined to the ...
Refinement of heavy-atom parameters
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.5, p. 848 [ doi:10.1107/97809553602060000899 ]
Refinement of heavy-atom parameters 25.1.2.5. Refinement of heavy-atom parameters Refinement of the heavy-atom parameters was first performed by the use of Rollett's (1961) least-squares program on the MERCURY computer, using the values as structure amplitudes. This procedure gave satisfactory results for the K2HgI4, K2PdCl4 and MHTS ...
Other potential derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.4, pp. 847-848 [ doi:10.1107/97809553602060000899 ]
Other potential derivatives 25.1.2.4.4. Other potential derivatives As is usual in protein work, RJP tried many other heavy-atom compounds (Poljak, 1963), but none gave useful results. In particular, a uranyl derivative, obtained by the use of UO2NO3, gave difference-Patterson maps that were difficult to interpret, and it was not ...
The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.3, p. 847 [ doi:10.1107/97809553602060000899 ]
The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative 25.1.2.4.3. The o-mercurihydroxytoluene p-sulfonate (MHTS) derivative The hk0 difference-Patterson map of the p-mercuribenzene sulfonate (PCMBS) derivative was interpretable in terms of a single site of substitution at 8Å resolution, but it was not useful beyond about 8 Å because of lack ...
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