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Protein chemistry of heavy-atom reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5, pp. 321-324 [ doi:10.1107/97809553602060000837 ]
... properties and are generally used as nitrates, acetates or chlorides (Blundell & Johnson, 1976; Carvin, 1986). The lanthanide contraction, a steady ... are given in Table 12.1.5.3. The covalent character in Hg-L bonds, especially in the two-coordinate complexes, can cause solubility ... species and I-. An oxidizing agent, such as chloramine T, can be added to KI, typically in a concentration ...
Iodine
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.6, p. 324 [ doi:10.1107/97809553602060000837 ]
... species and I-. An oxidizing agent, such as chloramine T, can be added to KI, typically in a concentration ratio ...
Hydrophobic heavy-atom reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.5, pp. 323-324 [ doi:10.1107/97809553602060000837 ]
Hydrophobic heavy-atom reagents 12.1.5.5. Hydrophobic heavy-atom reagents Since many heavy-atom reagents are hydrophilic, most interactions occur at the protein surface. However, substitution, addition or removal of the non-heavy-atom component(s) of the reagent can alter the hydrophilic-hydrophobic balance and lead to penetration of the core. ...
Electrostatic binding of heavy-atom anions
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.4, p. 323 [ doi:10.1107/97809553602060000837 ]
Electrostatic binding of heavy-atom anions 12.1.5.4. Electrostatic binding of heavy-atom anions Positively charged groups of proteins, such as the [alpha]-amino terminus, -amino of lysine, guanidinium of arginine and imadazolium of histidine, may form ion pairs with heavy-atom anionic complexes. For example, and can bind through electrostatic interactions. ...
B-metal reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.3, pp. 321-323 [ doi:10.1107/97809553602060000837 ]
... are given in Table 12.1.5.3. The covalent character in Hg-L bonds, especially in the two-coordinate complexes, can cause solubility ... Sasaki, K., Dockerill, S., Adamiak, D. A., Tickle, I. J. & Blundell, T. L. (1975). X-ray analysis of glucagon and ...
Thallium and lead ions
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.2, p. 321 [ doi:10.1107/97809553602060000837 ]
Thallium and lead ions 12.1.5.2. Thallium and lead ions Thallium and lead can provide useful derivatives, especially in their lower oxidation states, Tl(I) and Pb(II), when they resemble class A metals. Owing to the non-group valence and presence of an inert pair of electrons, the ionic radii of ...
Hard cations
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.1, p. 321 [ doi:10.1107/97809553602060000837 ]
... properties and are generally used as nitrates, acetates or chlorides (Blundell & Johnson, 1976; Carvin, 1986). The lanthanide contraction, a steady ... acetate may enable a useful derivative to be obtained. References Blundell, T. L. & Johnson, L. N. (1976). Protein Crystallography. New ...
Polynuclear reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.7, p. 324 [ doi:10.1107/97809553602060000837 ]
... reviewed by Thygesen et al. (1996). References O'Halloran, T. V., Lippard, S. J., Richmond, T. J. & Klug, A. (1987). Multiple heavy-atom reagents for ...
International Tables for Crystallography (2012). Vol. F, Section 12.1.5, pp. 321-324 [ doi:10.1107/97809553602060000837 ]
... properties and are generally used as nitrates, acetates or chlorides (Blundell & Johnson, 1976; Carvin, 1986). The lanthanide contraction, a steady ... are given in Table 12.1.5.3. The covalent character in Hg-L bonds, especially in the two-coordinate complexes, can cause solubility ... species and I-. An oxidizing agent, such as chloramine T, can be added to KI, typically in a concentration ...
Iodine
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.6, p. 324 [ doi:10.1107/97809553602060000837 ]
... species and I-. An oxidizing agent, such as chloramine T, can be added to KI, typically in a concentration ratio ...
Hydrophobic heavy-atom reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.5, pp. 323-324 [ doi:10.1107/97809553602060000837 ]
Hydrophobic heavy-atom reagents 12.1.5.5. Hydrophobic heavy-atom reagents Since many heavy-atom reagents are hydrophilic, most interactions occur at the protein surface. However, substitution, addition or removal of the non-heavy-atom component(s) of the reagent can alter the hydrophilic-hydrophobic balance and lead to penetration of the core. ...
Electrostatic binding of heavy-atom anions
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.4, p. 323 [ doi:10.1107/97809553602060000837 ]
Electrostatic binding of heavy-atom anions 12.1.5.4. Electrostatic binding of heavy-atom anions Positively charged groups of proteins, such as the [alpha]-amino terminus, -amino of lysine, guanidinium of arginine and imadazolium of histidine, may form ion pairs with heavy-atom anionic complexes. For example, and can bind through electrostatic interactions. ...
B-metal reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.3, pp. 321-323 [ doi:10.1107/97809553602060000837 ]
... are given in Table 12.1.5.3. The covalent character in Hg-L bonds, especially in the two-coordinate complexes, can cause solubility ... Sasaki, K., Dockerill, S., Adamiak, D. A., Tickle, I. J. & Blundell, T. L. (1975). X-ray analysis of glucagon and ...
Thallium and lead ions
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.2, p. 321 [ doi:10.1107/97809553602060000837 ]
Thallium and lead ions 12.1.5.2. Thallium and lead ions Thallium and lead can provide useful derivatives, especially in their lower oxidation states, Tl(I) and Pb(II), when they resemble class A metals. Owing to the non-group valence and presence of an inert pair of electrons, the ionic radii of ...
Hard cations
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.1, p. 321 [ doi:10.1107/97809553602060000837 ]
... properties and are generally used as nitrates, acetates or chlorides (Blundell & Johnson, 1976; Carvin, 1986). The lanthanide contraction, a steady ... acetate may enable a useful derivative to be obtained. References Blundell, T. L. & Johnson, L. N. (1976). Protein Crystallography. New ...
Polynuclear reagents
International Tables for Crystallography (2012). Vol. F, Section 12.1.5.7, p. 324 [ doi:10.1107/97809553602060000837 ]
... reviewed by Thygesen et al. (1996). References O'Halloran, T. V., Lippard, S. J., Richmond, T. J. & Klug, A. (1987). Multiple heavy-atom reagents for ...
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