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Results for DC.creator="C." AND DC.creator="A." AND DC.creator="Vernon" in section 25.1.2 of volume F page 2 of 2 pages. |
The palladium chloride (K2PdCl4) derivative
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.2, p. 847 [ doi:10.1107/97809553602060000899 ]
... chloride (K2PdCl4) derivative An attempt to use K2PtCl4 to produce a useful derivative gave disordered crystals, but a substitute for it was found by soaking crystals in K2PdCl4 at a molar ratio of 3:1 relative to lysozyme. Despite ...
The mercuri-iodide (K2HgI4) derivative
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.1, p. 847 [ doi:10.1107/97809553602060000899 ]
... several levels of substitution, RJP used the K2HgI4 salt at a molar concentration eight to ten times that of lysozyme. Based ... contains two methionine residues per molecule, and in keeping with a suggestion of Bluhm et al. (1958), RJP was expecting to ... the hk0 difference-Patterson map was interpretable in terms of a single site of substitution. This site, however, was very ...
Determination of heavy-atom positions
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4, pp. 847-848 [ doi:10.1107/97809553602060000899 ]
... 110) and (001) planes. In principle, all three coordinates of a heavy atom can be determined from projections on (100) or ... time to time by the use of Beevers-Lipson strips - a less demanding task than it might appear, since only about ... several levels of substitution, RJP used the K2HgI4 salt at a molar concentration eight to ten times that of lysozyme. ...
Preparation of heavy-atom derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.3, pp. 846-847 [ doi:10.1107/97809553602060000899 ]
... RJP, lysozyme crystals were grown in glass vials in which a 1 ml solution contained between 20 and 50 mg of ... with those from the native protein by superimposing them on a light box. This showed immediately whether the cell dimensions had ... conditions for the preparation of derivatives with high occupancy of a small number of sites. In this way it was ...
Lysozyme crystallization
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.2, p. 846 [ doi:10.1107/97809553602060000899 ]
... water at concentrations ranging from 50 to 100mgml-1. To a volume of the lysozyme solution, an equal volume of 10 ... 0.5 to 1mm3, grew overnight or during the course of a few days. The crystals were modified bipyramids with well developed ... shape. Precession photographs confirmed that the unit-cell dimensions were a = b = 79.1Å and c = 37.9Å, and that the space ...
Technical facilities
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.1, p. 845 [ doi:10.1107/97809553602060000899 ]
... been built in the laboratory to the design of D. A. G. Broad (patent 1956) under the direction of U. W. Arndt. We had a number of Buerger precession cameras and a Joyce-Loebl scanning densitometer, which had been used in ...
The electron-density map of lysozyme at 6Å resolution
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.8, pp. 853-854 [ doi:10.1107/97809553602060000899 ]
... distribution was calculated on the MERCURY computer, by means of a program written by Owen Mills that was in general use ... distribution in lysozyme at 6Å resolution viewed parallel to the c axis. The horizontal and vertical lines represent the twofold rotation ... in studying this map was to determine the boundary of a single molecule. Comparison of the unit cells of various ...
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.2, p. 847 [ doi:10.1107/97809553602060000899 ]
... chloride (K2PdCl4) derivative An attempt to use K2PtCl4 to produce a useful derivative gave disordered crystals, but a substitute for it was found by soaking crystals in K2PdCl4 at a molar ratio of 3:1 relative to lysozyme. Despite ...
The mercuri-iodide (K2HgI4) derivative
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4.1, p. 847 [ doi:10.1107/97809553602060000899 ]
... several levels of substitution, RJP used the K2HgI4 salt at a molar concentration eight to ten times that of lysozyme. Based ... contains two methionine residues per molecule, and in keeping with a suggestion of Bluhm et al. (1958), RJP was expecting to ... the hk0 difference-Patterson map was interpretable in terms of a single site of substitution. This site, however, was very ...
Determination of heavy-atom positions
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.4, pp. 847-848 [ doi:10.1107/97809553602060000899 ]
... 110) and (001) planes. In principle, all three coordinates of a heavy atom can be determined from projections on (100) or ... time to time by the use of Beevers-Lipson strips - a less demanding task than it might appear, since only about ... several levels of substitution, RJP used the K2HgI4 salt at a molar concentration eight to ten times that of lysozyme. ...
Preparation of heavy-atom derivatives
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.3, pp. 846-847 [ doi:10.1107/97809553602060000899 ]
... RJP, lysozyme crystals were grown in glass vials in which a 1 ml solution contained between 20 and 50 mg of ... with those from the native protein by superimposing them on a light box. This showed immediately whether the cell dimensions had ... conditions for the preparation of derivatives with high occupancy of a small number of sites. In this way it was ...
Lysozyme crystallization
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.2, p. 846 [ doi:10.1107/97809553602060000899 ]
... water at concentrations ranging from 50 to 100mgml-1. To a volume of the lysozyme solution, an equal volume of 10 ... 0.5 to 1mm3, grew overnight or during the course of a few days. The crystals were modified bipyramids with well developed ... shape. Precession photographs confirmed that the unit-cell dimensions were a = b = 79.1Å and c = 37.9Å, and that the space ...
Technical facilities
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.1, p. 845 [ doi:10.1107/97809553602060000899 ]
... been built in the laboratory to the design of D. A. G. Broad (patent 1956) under the direction of U. W. Arndt. We had a number of Buerger precession cameras and a Joyce-Loebl scanning densitometer, which had been used in ...
The electron-density map of lysozyme at 6Å resolution
International Tables for Crystallography (2012). Vol. F, Section 25.1.2.8, pp. 853-854 [ doi:10.1107/97809553602060000899 ]
... distribution was calculated on the MERCURY computer, by means of a program written by Owen Mills that was in general use ... distribution in lysozyme at 6Å resolution viewed parallel to the c axis. The horizontal and vertical lines represent the twofold rotation ... in studying this map was to determine the boundary of a single molecule. Comparison of the unit cells of various ...
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