International
Tables for
Crystallography
Volume C
Mathematical, physical and chemical tables
Edited by E. Prince

International Tables for Crystallography (2006). Vol. C. ch. 7.3, p. 652

Section 7.3.7.3. Position-sensitive detectors

P. Converta and P. Chieuxa

a Institut Laue–Langevin, Avenue des Martyrs, BP 156X, F-38042 Grenoble CEDEX, France

7.3.7.3. Position-sensitive detectors

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  • (a) Calibration of the position. For multi-electrode PSDs, the relative position of the electrodes is fixed and verified at the time of construction. In the case of other PSDs with analogue encoding, an angular calibration is made periodically with the help of a Bragg pattern, a thin neutron beam, or a cadmium mask moved across a diffuse beam incident on the PSD (Berliner, Mildner, Sudol & Taub, 1983[link]).

  • (b) Calibration of the PSD homogeneity. The response function might be dependent on the position within the PSD and possibly on the intensities collected at other parts of the PSD. The homogeneity of response of a PSD, which is normally better than 5%, can be calibrated to a much higher accuracy, since the stability of the PSDs is generally very good (e.g. 0.1% or better for gas PSDs). In the case of a reactor, the classical method of calibration is the use of an isotropic scatterer such as vanadium. The calibration is made at angles that avoid the very small vanadium Bragg peaks (or with displacement of the PSD to several positions) and that keep a low and isotropic background. Calibration factors, sometimes called cell-efficiency coefficients αi, are then obtained. Considering the lack of isotropy of the vanadium pattern, this method is limited to about 1% accuracy. For small PSDs, a precision of 0.1% or better is obtainable by scanning the whole PSD with a step equal to the cell spacing through any nearly isotropic pattern.

  • (c) Particular effects due to high intensities. The dead time of a PSD is complex. It depends on multiple parameters (the independent amplifiers and the encoding–decoding procedure). However, if there is a unique decoding logic for the whole PSD, and if this gives the highest contribution to the dead time, the ratios of the peak intensities are then conserved. In the case of strong Bragg peaks, the parasitic effect of scattering by the PSD entrance window (e.g. 10 mm aluminium for high-pressure gas PSDs) is detectable and can be corrected after calibration (using an intense and well localized thin beam).

References

First citation Berliner, R., Mildner, D. F. R., Sudol, J. & Taub, H. (1983). Position-sensitive detectors and data collection systems at the University of Missouri Research Reactor Facility. Position-sensitive detection of thermal neutrons, edited by P. Convert & J. B. Forsyth, pp. 120–128. London: Academic Press.Google Scholar








































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