International
Tables for Crystallography Volume F Crystallography of biological macromolecules Edited by M. G. Rossmann and E. Arnold © International Union of Crystallography 2006 |
International Tables for Crystallography (2006). Vol. F. ch. 6.1, p. 125
|
A section through a permanently evacuated, sealed X-ray tube is shown in Fig. 6.1.2.1 The tube has a spirally wound tungsten filament, F, placed immediately behind a slot in the focusing cup, C, and a water-cooled target or anode, T, approximately 10 mm from the surface of C. The filament–focusing-cup assembly is at a negative voltage of between 30 and 50 kV, and the target is at ground potential. The electron beam strikes the target in a focal line, which acts as a line source of X-rays. There are usually two pairs of X-ray windows, W, through which the source is viewed at a small angle to the target surface, thus producing a foreshortened effective source, X, which is approximately square in one plane and a narrow line in the other. Focus dimensions on the target and maximum recommended power loading are shown for a number of standard inserts in Table 6.1.2.1. None of these are ideal for macromolecular crystallography. The assembly of a cathode, anode and windows – the tube insert – is inserted in a shock- and radiation-proof shield which is fixed to the table. Attached to the shield are X-ray shutters and filters, and sometimes brackets for bolting on X-ray cameras. A high-voltage connection is made to the tube by means of a flexible, shielded, shock-proof cable; nowadays, this high voltage is almost invariably full-wave rectified and smoothed DC.
|