International
Tables for
Crystallography
Volume C
Mathematical, physical and chemical tables
Edited by E. Prince

International Tables for Crystallography (2006). Vol. C. ch. 2.2, p. 35

Section 2.2.5.1. General

J. R. Helliwella

a Department of Chemistry, University of Manchester, Manchester M13 9PL, England

2.2.5.1. General

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The precession method is used to record an undistorted representation of a single plane of relp's and their associated intensities. In order to achieve this, the crystal is carefully set so that the plane of relp's is perpendicular to the X-ray beam. The normal to this plane, the zone axis, is then precessed about the X-ray-beam axis. A layer-line screen allows only relp's of the plane of interest to pass through to the film. The motion of the crystal, screen, and film are coupled together to maintain the coplanarity of the film, screen, and zone.








































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