International Tables for Crystallography (2006). Vol. C. ch. 2.2, pp. 26-41
https://doi.org/10.1107/97809553602060000577 |
Chapter 2.2. Single-crystal X-ray techniques
Contents
- 2.2. Single-crystal X-ray techniques (pp. 26-41) | html | pdf | chapter contents |
- 2.2.1. Laue geometry (pp. 26-29) | html | pdf |
- 2.2.1.1. General (pp. 26-27) | html | pdf |
- 2.2.1.2. Crystal setting (p. 27) | html | pdf |
- 2.2.1.3. Single-order and multiple-order reflections (pp. 27-29) | html | pdf |
- 2.2.1.4. Angular distribution of reflections in Laue diffraction (p. 29) | html | pdf |
- 2.2.1.5. Gnomonic and stereographic transformations (p. 29) | html | pdf |
- 2.2.2. Monochromatic methods (pp. 29-30) | html | pdf |
- 2.2.3. Rotation/oscillation geometry (pp. 31-34) | html | pdf |
- 2.2.3.1. General (p. 31) | html | pdf |
- 2.2.3.2. Diffraction coordinates (pp. 31-33) | html | pdf |
- 2.2.3.3. Relationship of reciprocal-lattice coordinates to crystal system parameters (p. 33) | html | pdf |
- 2.2.3.4. Maximum oscillation angle without spot overlap (pp. 33-34) | html | pdf |
- 2.2.3.5. Blind region (p. 34) | html | pdf |
- 2.2.4. Weissenberg geometry (pp. 34-35) | html | pdf |
- 2.2.5. Precession geometry (pp. 35-36) | html | pdf |
- 2.2.6. Diffractometry (pp. 36-37) | html | pdf |
- 2.2.7. Practical realization of diffraction geometry: sources, optics, and detectors (pp. 37-41) | html | pdf |
- 2.2.7.1. General (p. 37) | html | pdf |
- 2.2.7.2. Conventional X-ray sources: spectral character, crystal rocking curve, and spot size (pp. 37-38) | html | pdf |
- 2.2.7.3. Synchrotron X-ray sources (pp. 38-41) | html | pdf |
- 2.2.7.4. Geometric effects and distortions associated with area detectors (p. 41) | html | pdf |
- References | html | pdf |
- Figures
- Fig. 2.2.1.1. Laue geometry (p. 27) | html | pdf |
- Fig. 2.2.1.2. A predicted Laue pattern of a protein crystal with a zone axis parallel to the incident, polychromatic X-ray beam (p. 27) | html | pdf |
- Fig. 2.2.1.3. A multiple component spot in Laue geometry (p. 28) | html | pdf |
- Fig. 2.2.1.4. The variation with M = λmax/λmin of the proportions of relp's lying on single, double, and triple rays for the case (p. 28) | html | pdf |
- Fig. 2.2.1.5. Geometrical principles of the spherical, stereographic, gnomonic, and Laue projections (p. 29) | html | pdf |
- Fig. 2.2.3.1. (a) Elevation of the sphere of reflection (p. 30) | html | pdf |
- Fig. 2.2.3.2. Geometrical principles of recording the pattern on (a) a plane detector, (b) a V-shaped detector, (c) a cylindrical detector (p. 31) | html | pdf |
- Fig. 2.2.3.3. The rotation method. Definition of coordinate systems (p. 32) | html | pdf |
- Fig. 2.2.3.4. The rotation method. The blind region associated with a single rotation axis (p. 33) | html | pdf |
- Fig. 2.2.5.1. The screenless precession setting photograph (schematic) and associated mis-setting angles for a typical orientation error when the crystal has been set previously by a monochromatic still or Laue (p. 35) | html | pdf |
- Fig. 2.2.6.1. Normal-beam equatorial geometry: the angles ω, χ, φ, 2θ are drawn in the convention of Hamilton (1974) (p. 36) | html | pdf |
- Fig. 2.2.6.2. Diffractometry with normal-beam equatorial geometry and angular motions ω, χ and φ (p. 36) | html | pdf |
- Fig. 2.2.7.1. Reflection rocking width for a conventional X-ray source (p. 38) | html | pdf |
- Fig. 2.2.7.2. Single-crystal monochromator illuminated by synchrotron radiation: (a) flat crystal, (b) Guinier setting, (c) overbent crystal, (d) effect of source size (shown at the Guinier setting for clarity) (p. 39) | html | pdf |
- Fig. 2.2.7.3. Double-crystal monochromator illuminated by synchrotron radiation (p. 40) | html | pdf |
- Fig. 2.2.7.4. The rocking width of an individual reflection for the case of Fig. 2.2.7.2(c) and a vertical rotation axis (p. 40) | html | pdf |
- Tables
- Table 2.2.3.1. Glossary of symbols used to specify quantities on diffraction patterns and in reciprocal space (p. 32) | html | pdf |
- Table 2.2.5.1. The distance displacement (in mm) measured on the film versus angular setting error of the crystal for a screenless precession () setting photograph (p. 35) | html | pdf |
- 2.2.1. Laue geometry (pp. 26-29) | html | pdf |