International Tables for Crystallography (2019). Vol. H. ch. 2.9, pp. 189-199
https://doi.org/10.1107/97809553602060000944

Chapter 2.9. Cells for in situ powder-diffraction investigation of chemical reactions

Contents

  • 2.9. Cells for in situ powder-diffraction investigation of chemical reactions  (pp. 189-199) | html | pdf | chapter contents |
    W. van Beek and P. Pattison
    • 2.9.1. Introduction  (p. 189) | html | pdf |
    • 2.9.2. Historical perspective  (p. 189) | html | pdf |
    • 2.9.3. Main types of reaction cells  (pp. 189-197) | html | pdf |
      • 2.9.3.1. Introduction  (p. 189) | html | pdf |
      • 2.9.3.2. Capillary cells  (pp. 189-192) | html | pdf |
      • 2.9.3.3. Reactions requiring specialist cells  (pp. 192-195) | html | pdf |
        • 2.9.3.3.1. Cells for electrochemistry  (pp. 192-193) | html | pdf |
        • 2.9.3.3.2. Cells with humidity control  (pp. 193-194) | html | pdf |
        • 2.9.3.3.3. Large-volume cells for energy-dispersive diffraction  (p. 194) | html | pdf |
        • 2.9.3.3.4. Large-volume cells for angular-dispersive diffraction  (pp. 194-195) | html | pdf |
      • 2.9.3.4. Cells specifically for neutrons  (pp. 195-197) | html | pdf |
        • 2.9.3.4.1. Introduction  (pp. 195-196) | html | pdf |
        • 2.9.3.4.2. Solid–gas reactions  (p. 196) | html | pdf |
        • 2.9.3.4.3. Electrochemistry using neutron diffraction  (p. 196) | html | pdf |
        • 2.9.3.4.4. Hydrothermal reaction cells  (pp. 196-197) | html | pdf |
    • 2.9.4. Complementary methods and future developments  (p. 197) | html | pdf |
    • References | html | pdf |
    • Figures
      • Fig. 2.9.1. (a) Swagelock VCR gland with an epoxy-glued capillary (red ellipse)  (p. 190) | html | pdf |
      • Fig. 2.9.2. (a) An exploded representation of the flow-cell/furnace components, indicating how they fit together  (p. 190) | html | pdf |
      • Fig. 2.9.3. Sketch of a typical experimental setup and a three-dimensional drawing of the in situ flow cell  (p. 191) | html | pdf |
      • Fig. 2.9.4. (a) In situ three-dimensional stacked plot of the intercalation of ibuprofen into an LDH  (p. 191) | html | pdf |
      • Fig. 2.9.5. (a) In situ synchrotron diffraction patterns (selected region) of an LiCoO2/Li cell collected during cell charging  (p. 192) | html | pdf |
      • Fig. 2.9.6. Schematic drawing of the humidity-control system: (1) mass-flow controller, (2) adsorption dryer, (3) pressure regulator, (4) heated bubbler, (5) peristaltic pump, (6) water reservoir, (7) thermostat, (8) condensation trap, (9) mixing chamber and (10) thermostat  (p. 193) | html | pdf |
      • Fig. 2.9.7. Sequence of XRD measurements between 21 and 27° 2θ  (p. 193) | html | pdf |
      • Fig. 2.9.8. A schematic of the Oxford/Daresbury hydrothermal autoclave used for energy-dispersive X-ray diffraction studies  (p. 194) | html | pdf |
      • Fig. 2.9.9. (a) Schematic of a sodium-halide cell in an in situ synchrotron EDXRD experimental setup  (p. 195) | html | pdf |